Preparation and Characterization of Derivatives of Pyrimidines in two ways Clascical and Microwave

AL-Hiti, Waleed; J.Khammase, Samea; T.Mahdi, Bushra

doi:10.37652/juaps.2016.135152

Document Type : Research Paper

Authors

¹ University Of Anbar- College of Education for Women

² University of Baghdad - College of Science for Women

³ University Of Anbar- College of Education for Women.

https://doi.org/10.37652/juaps.2016.135152

Abstract

This study includes synthesis and characterization of new pyrimidine derivatives (R or Ar-2,3,4,6,7,8-hexahydroquinazolin-5(1H)-one), via of the reaction from cyclohexane-1,3-dione with aldehyde derivatives and guanidinehydrochlorid. Usingabsolute ethanol as a solvent .This mixture was refluxed for (4 – 6) hrs;While maintaining the pH at 6. The same derivatives of pyrimidine were prepared in microwave waytechnique.The prepared compounds were characterized by melting point , FT-IR , UV-Vis 1H-NMR and 13C-NMR spectroscopy

Keywords

Main Subjects

Chemistry

References

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Journal of University of Anbar for Pure Science

Preparation and Characterization of Derivatives of Pyrimidines in two ways Clascical and Microwave

References

References

Volume 10, Issue 3
December 2016
Page 22-34

Preparation and Characterization of Derivatives of Pyrimidines in two ways Clascical and Microwave

References

References

Volume 10, Issue 3December 2016Page 22-34

Volume 10, Issue 3
December 2016
Page 22-34